An Introductory Course of Quantitative Chemical Analysis

Contents

• PREFACE

• PART I. INTRODUCTION

  SUBDIVISIONS OF ANALYTICAL CHEMISTRY

  GENERAL DIRECTIONS
    Accuracy and Economy of Time; Notebooks; Reagents; Wash-bottles; Transfer of Liquids

• PART II. VOLUMETRIC ANALYSIS

  GENERAL DISCUSSION
    Subdivisions; The Analytical Balance; Weights; Burettes; Calibration of Measuring Devices

  GENERAL DIRECTIONS
    Standard and Normal Solutions

  I. Neutralization Methods

  ALKALIMETRY AND ACIDIMETRY
    Preparation and Standardization of Solutions; Indicators

  STANDARDIZATION OF HYDROCHLORIC ACID

  DETERMINATION OF TOTAL ALKALINE STRENGTH OF SODA ASH

  DETERMINATION OF ACID STRENGTH OF OXALIC ACID

  II. Oxidation Processes

  GENERAL DISCUSSION
    BICHROMATE PROCESS FOR THE DETERMINATION OF IRON
    DETERMINATION OF IRON IN LIMONITE BY THE BICHROMATE PROCESS
    DETERMINATION OF CHROMIUM IN CHROME IRON ORE
    PERMANGANATE PROCESS FOR THE DETERMINATION OF IRON
    DETERMINATION OF IRON IN LIMONITE BY THE PERMANGANATE PROCESS
    DETERMINATION OF IRON IN LIMONITE BY THE ZIMMERMANN-REINHARDT PROCESS
    DETERMINATION OF THE OXIDIZING POWER OF PYROLUSITE
    IODIMETRY
    DETERMINATION OF COPPER IN ORES
    DETERMINATION OF ANTIMONY IN STIBNITE
    CHLORIMETRY
    DETERMINATION OF AVAILABLE CHLORINE IN BLEACHING POWDER

  III. Precipitation Methods

  DETERMINATION OF SILVER BY THE THIOCYANATE PROCESS

• PART III. GRAVIMETRIC ANALYSIS

  GENERAL DIRECTIONS
    Precipitation; Funnels and Filters; Filtration and Washing of Precipitates; Desiccators; Crucibles and their Preparation for Use; Ignition of Precipitates
  DETERMINATION OF CHLORINE IN SODIUM CHLORIDE
  DETERMINATION OF IRON AND OF SULPHUR IN FERROUS AMMONIUM SULPHATE
  DETERMINATION OF SULPHUR IN BARIUM SULPHATE
  DETERMINATION OF PHOSPHORIC ANHYDRIDE IN APATITE
  ANALYSIS OF LIMESTONE
    Determination of Moisture; Insoluble Matter and Silica; Ferric Oxide and Alumina; Calcium; Magnesium; Carbon Dioxide
  ANALYSIS OF BRASS
    Electrolytic Separations; Determination of Lead, Copper, Iron and Zinc.
  DETERMINATION OF SILICA IN SILICATES

• PART IV. STOICHIOMETRY

  SOLUTIONS OF TYPICAL PROBLEMS
  PROBLEMS

• APPENDIX

  ELECTROLYTIC DISSOCIATION THEORY
  FOLDING OF A FILTER PAPER
  SAMPLE NOTEBOOK PAGES
  STRENGTH OF REAGENTS
  DENSITIES AND VOLUMES OF WATER
  CORRECTIONS FOR CHANGE OF TEMPERATURE OF STANDARD SOLUTIONS
  ATOMIC WEIGHTS
  LOGARITHM TABLES

• INDEX